4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide

Base Information

Chemical Name:4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide
CAS No.:1418128-61-6
Molecular Formula:C₄₀H₅₀BNO₄Si
Molecular Weight:647.738
Hs Code.:

Synonyms:4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide

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Chemical Property of 4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide

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Technology Process of 4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide

There total 5 articles about 4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1418128-59-2
2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine

: 1710-98-1
p-tert-butyl benzoyl chloride

: 1418128-61-6
4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1.08333h;

Reference yield:

: 861106-91-4
(2-bromo-6-nitro-phenyl)-methanol

: 1418128-61-6
4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 - 50 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 4 h / 90 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 h / 20 °C / 760.05 Torr

4: triethylamine / dichloromethane / 1.08 h / 0 - 20 °C

With 1H-imidazole; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; hydrogen; potassium acetate; triethylamine; In 1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1418128-54-7
(2-bromo-6-nitro-benzyloxy)-tert-butyl-diphenyl-silane

: 1418128-61-6
4-tert-butyl-N-[(2-tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 4 h / 90 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 h / 20 °C / 760.05 Torr

3: triethylamine / dichloromethane / 1.08 h / 0 - 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; hydrogen; potassium acetate; triethylamine; In 1,4-dioxane; dichloromethane; ethyl acetate;