4-formyl-3,5-dimethoxyphenyl ester

Base Information

Chemical Name:4-formyl-3,5-dimethoxyphenyl ester
CAS No.:1373512-12-9
Molecular Formula:C₁₃H₁₄O₆
Molecular Weight:266.251
Hs Code.:

Synonyms:4-formyl-3,5-dimethoxyphenyl ester

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Chemical Property of 4-formyl-3,5-dimethoxyphenyl ester

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Technology Process of 4-formyl-3,5-dimethoxyphenyl ester

There total 1 articles about 4-formyl-3,5-dimethoxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 22080-96-2
syringaldehyde

: 2937-50-0
Allyl chloroformate

: 1373512-12-9
4-formyl-3,5-dimethoxyphenyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 23 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo300400q

Reference yield:

: 1373512-12-9
4-formyl-3,5-dimethoxyphenyl ester

: 4-(2-tert-butylphenoxymethyl)-3,5-dimethoxyphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / methanol; dichloromethane / 0.08 h / Inert atmosphere

2.1: tributylphosphine; diamide / benzene / 0.25 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 - 23 °C / Inert atmosphere

With sodium tetrahydroborate; tributylphosphine; diamide; In methanol; dichloromethane; benzene;
DOI:10.1021/jo300400q