C₃₁H₄₄O₆Si

Base Information

Chemical Name:C₃₁H₄₄O₆Si
CAS No.:1032880-04-8
Molecular Formula:C₃₁H₄₄O₆Si
Molecular Weight:540.772
Hs Code.:

C<sub>31</sub>H<sub>44</sub>O<sub>6</sub>Si

Synonyms:C₃₁H₄₄O₆Si

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Chemical Property of C₃₁H₄₄O₆Si

Chemical Property:

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Technology Process of C₃₁H₄₄O₆Si

There total 11 articles about C₃₁H₄₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1032880-02-6
C₂₉H₄₀O₆Si

: 1826-67-1
vinyl magnesium bromide

: 1032880-04-8
C₃₁H₄₄O₆Si

: 1032880-06-0
C₃₁H₄₄O₆Si

Guidance literature:: C₂₉H₄₀O₆Si; vinyl magnesium bromide; In tetrahydrofuran; at -78 ℃; for 1h;

With sodium hydrogencarbonate; In tetrahydrofuran; water;
DOI:10.1021/ol8008057

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1032880-04-8
C₃₁H₄₄O₆Si

: 1032880-06-0
C₃₁H₄₄O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / tetrahydrofuran / -10 - 20 °C

1.2: 2 h / -10 - 20 °C

2.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

3.1: (-)-B-methoxydiisopinocamphenylborane / diethyl ether / 1 h / 0 - 20 °C

3.2: 3 h / -78 °C

4.1: sodium hydride / tetrahydrofuran / 1 h / -10 - 20 °C

4.2: 12 h / 20 °C

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

5.2: 2 h / Reflux

6.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

7.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1 h / -10 - 20 °C

8.1: toluene-4-sulfonic acid / dichloromethane / 3 h / 0 - 20 °C

9.1: pyridine; dmap / dichloromethane / 20 °C

10.1: tetrahydrofuran / 1 h / -78 °C

With pyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; (-)-B-methoxydiisopinocamphenylborane; sulfur trioxide pyridine complex; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)54

Reference yield:

: 136032-73-0,127251-09-6
4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-L-threitol

: 1032880-04-8
C₃₁H₄₄O₆Si

: 1032880-06-0
C₃₁H₄₄O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

2.1: (-)-B-methoxydiisopinocamphenylborane / diethyl ether / 1 h / 0 - 20 °C

2.2: 3 h / -78 °C

3.1: sodium hydride / tetrahydrofuran / 1 h / -10 - 20 °C

3.2: 12 h / 20 °C

4.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

4.2: 2 h / Reflux

5.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

6.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1 h / -10 - 20 °C

7.1: toluene-4-sulfonic acid / dichloromethane / 3 h / 0 - 20 °C

8.1: pyridine; dmap / dichloromethane / 20 °C

9.1: tetrahydrofuran / 1 h / -78 °C

With pyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; (-)-B-methoxydiisopinocamphenylborane; sulfur trioxide pyridine complex; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)54