1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester

Base Information

Chemical Name:1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester
CAS No.:1229006-19-2
Molecular Formula:C₁₈H₂₁NO₆
Molecular Weight:347.368
Hs Code.:

Synonyms:1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester

Suppliers and Price of 1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester

There total 10 articles about 1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119736-16-2
3-(benzyloxy)-1-((tert-butoxycarbonyl)amino)-4-oxo-1,4-dihydropyridine-2-carboxylic acid ethyl ester

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 74-88-4
methyl iodide

: 1229006-19-2
1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester

Guidance literature:: 3-(benzyloxy)-1-((tert-butoxycarbonyl)amino)-4-oxo-1,4-dihydropyridine-2-carboxylic acid ethyl ester; N,N-dimethyl-formamide dimethyl acetal; In ethanol; at 80 ℃; for 3h;

With acetic acid; In ethanol; at 20 ℃;

methyl iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol; N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 1229006-18-1
1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridine carboxylic acid

: 74-88-4
methyl iodide

: 1229006-19-2
1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester

Guidance literature:: With sodium hydrogencarbonate; In tert-butyl methyl ether; N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 118-71-8
Maltol

: 1229006-19-2
1-[2,2-bis(methyloxy)ethyl]-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetonitrile / 5 h / 13 - 80 °C / Large scale

2: bromobenzene; selenium(IV) oxide / 13 h / 140 °C / Dean-Stark

3: sodium chlorite; aminosulfonic acid / water; acetone / 0.67 h / 20 °C / Cooling with ice

4: ethanol / 18 h / 55 - 65 °C

5: sodium hydrogencarbonate; tert-butyl methyl ether / N,N-dimethyl-formamide / 20 °C

With selenium(IV) oxide; sodium chlorite; bromobenzene; tert-butyl methyl ether; aminosulfonic acid; sodium hydrogencarbonate; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide; acetone; acetonitrile;