Technology Process of C12H19BO3
There total 4 articles about C12H19BO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C12H17LiO;
With
Trimethyl borate;
In
tetrahydrofuran;
at -78 - 20 ℃;
With
hydrogenchloride;
In
tetrahydrofuran;
Further stages.;
DOI:10.1039/b008319o
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 91 percent / tetrabutylammonium tribromide / CHCl3
2.1: NaH / tetrahydrofuran / 0.5 h / 20 °C
2.2: 96 percent / tetrahydrofuran / 3 h / Heating
3.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C
4.1: trimethyl borate / tetrahydrofuran / -78 - 20 °C
4.2: 3.46 g / aq. HCl / tetrahydrofuran
With
n-butyllithium; Trimethyl borate; tetra-N-butylammonium tribromide; sodium hydride;
In
tetrahydrofuran; hexane; chloroform;
DOI:10.1039/b008319o
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: NaH / tetrahydrofuran / 0.5 h / 20 °C
1.2: 96 percent / tetrahydrofuran / 3 h / Heating
2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C
3.1: trimethyl borate / tetrahydrofuran / -78 - 20 °C
3.2: 3.46 g / aq. HCl / tetrahydrofuran
With
n-butyllithium; Trimethyl borate; sodium hydride;
In
tetrahydrofuran; hexane;
DOI:10.1039/b008319o