TH₀₃₈₂₁-148

Base Information

Chemical Name:TH₀₃₈₂₁-148
CAS No.:1431961-06-6
Molecular Formula:C₂₂H₃₄N₂O₄
Molecular Weight:390.523
Hs Code.:

Synonyms:TH₀₃₈₂₁-148

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Chemical Property of TH₀₃₈₂₁-148

Chemical Property:

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Technology Process of TH₀₃₈₂₁-148

There total 7 articles about TH₀₃₈₂₁-148 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431961-05-5
TH₀₃₈₂₁-134

: 1431961-06-6
TH₀₃₈₂₁-148

Guidance literature:: TH₀₃₈₂₁-134; In methanol; for 16h;

With palladium 10% on activated carbon; hydrogen; In methanol; for 16h; under 827.459 Torr;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1431961-06-6
TH₀₃₈₂₁-148

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 20 °C

2.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,4-dioxane / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

4.1: Raney Ni / methanol / 16 h

4.2: 16 h / 827.46 Torr

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; sodium carbonate; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 162356-90-3
N-(tert-butoxycarbonyl)-2-bromobenzylamine

: 1431961-06-6
TH₀₃₈₂₁-148

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,4-dioxane / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

3.1: Raney Ni / methanol / 16 h

3.2: 16 h / 827.46 Torr

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; sodium carbonate; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;