Technology Process of meso-monotriphenylporphyrin
There total 7 articles about meso-monotriphenylporphyrin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 85 percent / Et3N / diethyl ether / 1 h / Heating
2: 93 percent / n-BuLi, triphenylmethane / tetrahydrofuran; hexamethylphosphoric acid triamide / Ambient temperature
3: 82 percent / HCl / acetic acid / 1 h
4: SOCl2 / dimethylformamide / 0.42 h / Ambient temperature
5: 66 percent / dimethylformamide / 12 h
With
hydrogenchloride; n-butyllithium; thionyl chloride; triphenylmethane; triethylamine;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ja00532a033
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 97 percent / oxalyl chloride / benzene / 3 h / 50 °C
2: 85 percent / Et3N / diethyl ether / 1 h / Heating
3: 93 percent / n-BuLi, triphenylmethane / tetrahydrofuran; hexamethylphosphoric acid triamide / Ambient temperature
4: 82 percent / HCl / acetic acid / 1 h
5: SOCl2 / dimethylformamide / 0.42 h / Ambient temperature
6: 66 percent / dimethylformamide / 12 h
With
hydrogenchloride; n-butyllithium; thionyl chloride; oxalyl dichloride; triphenylmethane; triethylamine;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; acetic acid; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ja00532a033
