5'-O-acetyl-2',3'-dideoxy-O⁶-(2,4,6-triisopropylbenzenesulfonyl)inosine

Base Information

Chemical Name:5'-O-acetyl-2',3'-dideoxy-O⁶-(2,4,6-triisopropylbenzenesulfonyl)inosine
CAS No.:389128-13-6
Molecular Formula:C₂₇H₃₆N₄O₆S
Molecular Weight:544.672
Hs Code.:

5'-O-acetyl-2',3'-dideoxy-O<sup>6</sup>-(2,4,6-triisopropylbenzenesulfonyl)inosine

Synonyms:5'-O-acetyl-2',3'-dideoxy-O⁶-(2,4,6-triisopropylbenzenesulfonyl)inosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-acetyl-2',3'-dideoxy-O⁶-(2,4,6-triisopropylbenzenesulfonyl)inosine

Chemical Property:

Purity/Quality:

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Technology Process of 5'-O-acetyl-2',3'-dideoxy-O⁶-(2,4,6-triisopropylbenzenesulfonyl)inosine

There total 2 articles about 5'-O-acetyl-2',3'-dideoxy-O⁶-(2,4,6-triisopropylbenzenesulfonyl)inosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58-63-9
Inosine

: 389128-13-6
5'-O-acetyl-2',3'-dideoxy-O⁶-(2,4,6-triisopropylbenzenesulfonyl)inosine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2-acetoxyisobutyryl bromide / acetonitrile / 10 h / 20 °C

1.2: pyridine / 0.5 h / 20 °C

1.3: 146 mg / Zn-Cu; glacial acetic acid / tetrahydrofuran / 12 h / 20 °C

2.1: 72 percent / H₂; H₂O / Pd/C / methanol / 2 h

3.1: 12 percent / 4-DMAP; Et₃N / CH₂Cl₂ / 4 h / 20 °C

With dmap; acetoxyisobutyryl bromide; water; hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)00800-6

Reference yield:

: 130676-57-2
5'-O-acetyl-2',3'-didehydro-2',3'-dideoxyinosine

: 389128-13-6
5'-O-acetyl-2',3'-dideoxy-O⁶-(2,4,6-triisopropylbenzenesulfonyl)inosine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / H₂; H₂O / Pd/C / methanol / 2 h

2: 12 percent / 4-DMAP; Et₃N / CH₂Cl₂ / 4 h / 20 °C

With dmap; water; hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)00800-6