9-nitro-1,7-diphenyl-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinoline

Base Information

• Chemical Name: 9-nitro-1,7-diphenyl-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinoline
• CAS No.: 329082-03-3
• Molecular Formula: C₂₄H₂₂N₂O₂
• Molecular Weight: 370.451
• Mol file: 329082-03-3.mol

Synonyms:9-nitro-1,7-diphenyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinoline

Chemical Property of 9-nitro-1,7-diphenyl-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinoline

Chemical Property:

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Technology Process of 9-nitro-1,7-diphenyl-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinoline

There total 3 articles about 9-nitro-1,7-diphenyl-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-nitro-aniline (100-01-6,104810-17-5) → 9-nitro-1,7-diphenyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinoline (329082-03-3) + 6-nitro-4-phenyl-1,2,3,4-tetrahydroquinoline (1448444-05-0)

Guidance literature:

With 25,26,27,28-terahydroxycalix[4]arene-5,11,7,23-tetrasulfonic acid; In water; at 20 ℃; for 2h;

DOI:10.1039/c3ob40927a

Reference yield: 68.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-nitro-aniline (100-01-6,104810-17-5) → 9-nitro-1,7-diphenyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinoline (329082-03-3)

Guidance literature:

formaldehyd; 4-nitro-aniline; With silica sulfuric acid; In water; at 20 ℃; for 0.25h;

styrene; In water; for 24h; Reflux;

DOI:10.1002/jhet.4283

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 4-nitro-aniline (100-01-6,104810-17-5) → 9-nitro-1,7-diphenyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinoline (329082-03-3)

Guidance literature:

With formaldehyd; trifluoroacetic acid; In water; acetonitrile; at 20 ℃; Inert atmosphere; Heating; Reflux;

upstream raw materials:

styrene

4-nitro-aniline

formaldehyd

Downstream raw materials:

1,7-diphenyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinolin-9-amine

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