5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid

Base Information

Chemical Name:5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid
CAS No.:20725-32-0
Molecular Formula:C10H9N3O2
Molecular Weight:203.2
Hs Code.:2933990090
European Community (EC) Number:839-882-4
NSC Number:133540
DSSTox Substance ID:DTXSID20276169
Nikkaji Number:J962.159H
Wikidata:Q72495450
ChEMBL ID:CHEMBL1370586
Mol file:20725-32-0.mol

Synonyms:20725-32-0;5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid;5-Methyl-1-phenyl-1H-[1,2,3]triazole-4-carboxylic acid;5-methyl-1-phenyltriazole-4-carboxylic acid;5-methyl-1-phenyl-1,2,3-triazole-4-carboxylic acid;NSC133540;MLS000072666;SCHEMBL4771303;CHEMBL1370586;DTXSID20276169;RRHCZOBPABYIJZ-UHFFFAOYSA-N;HMS1681I04;HMS2280F07;HMS3435G06;MFCD00100217;STL139302;AKOS000301673;CCG-126867;NSC-133540;SMR000012942;TS-00352;BB 0242692;EN300-51795;AB00402395-04;AG-205/25006766;SR-01000369459;SR-01000369459-1;5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylicacid;F0346-0183;Z381397916;5-Methyl-1-phenyl-1H-[1,2,3]triazole-4-carbo xylic acid;0JI

Suppliers and Price of 5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Methyl-1-phenyl-1H-[1,2,3]triazole-4-carboxylicAcid
500mg
$ 200.00

Matrix Scientific
5-Methyl-1-phenyl-1H-[1,2,3]triazole-4-carboxylic acid
500mg
$ 182.00

Crysdot
5-Methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylicacid 95%
5g
$ 874.00

Atlantic Research Chemicals
5-Methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylicacid 95%
1gm:
$ 159.06

American Custom Chemicals Corporation
5-METHYL-1-PHENYL-1H-[1,2,3]TRIAZOLE-4-CARBOXYLIC ACID 95.00%
5G
$ 1252.83

American Custom Chemicals Corporation
5-METHYL-1-PHENYL-1H-[1,2,3]TRIAZOLE-4-CARBOXYLIC ACID 95.00%
2.5G
$ 1037.94

American Custom Chemicals Corporation
5-METHYL-1-PHENYL-1H-[1,2,3]TRIAZOLE-4-CARBOXYLIC ACID 95.00%
1G
$ 750.68

AK Scientific
5-Methyl-1-phenyl-1H-[1,2,3]triazole-4-carboxylicacid
500mg
$ 295.00

Total 8 raw suppliers

Chemical Property of 5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid

Chemical Property:

Vapor Pressure:2.91E-08mmHg at 25°C
Refractive Index:1.653
Boiling Point:432.9 °C at 760 mmHg
PKA:pK1:3.73 (25°C)
Flash Point:215.6 °C
PSA：68.01000
Density:1.35 g/cm³
LogP:1.27390
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:203.069476538
Heavy Atom Count:15
Complexity:241

Purity/Quality:

98%min ^*data from raw suppliers

5-Methyl-1-phenyl-1H-[1,2,3]triazole-4-carboxylicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(N=NN1C2=CC=CC=C2)C(=O)O

Technology Process of 5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid

There total 10 articles about 5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.9%

: 27049-64-5
5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid ethyl ester

: 20725-32-0
5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid

Guidance literature:: With sodium hydroxide; In ethanol; at 50 ℃; for 4h;
DOI:10.1016/j.bmc.2014.09.037

Reference yield: 84.0%

: 141-97-9
ethyl acetoacetate

: 622-37-7
Phenyl azide

: 20725-32-0
5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1134/S1070428008100217

Reference yield:

: 62-53-3
aniline

: 20725-32-0
5-methyl-1-phenyl-1H-1,2,3-triazole-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C

1.2: 0 - 5 °C

2.1: sodium ethanolate; ethanol

With hydrogenchloride; ethanol; sodium ethanolate; sodium nitrite; In water;