4-chlorophenyl diethyldithiophosphinate

Base Information

• Chemical Name: 4-chlorophenyl diethyldithiophosphinate
• CAS No.: 6078-99-5
• Molecular Formula: C₁₀H₁₄ClPS₂
• Molecular Weight: 264.78
• Mol file: 6078-99-5.mol

Synonyms:4-chlorophenyl diethyldithiophosphinate

Chemical Property of 4-chlorophenyl diethyldithiophosphinate

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of 4-chlorophenyl diethyldithiophosphinate

There total 12 articles about 4-chlorophenyl diethyldithiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tetraethyldiphosphine disulfide (3790-23-6) + C13H7Cl2NOS → 4-chlorophenyl diethyldithiophosphinate (6078-99-5) + 2-(diethylphosphinothioyl)-6-chlorobenzoxazole

Guidance literature:

With hydridotetakis(triphenylphosphine)rhodium(I); 1,2-bis[bis(4-methoxyphenyl)phosphanyl]ethane; In tetrahydrofuran; for 3h; Inert atmosphere; Reflux;

DOI:10.1002/adsc.201800630

Reference yield: 99.0%

tetraethyldiphosphine disulfide (3790-23-6) + 5-chloro-2-((4-chlorophenyl)thio)benzo[d]thiazole → 4-chlorophenyl diethyldithiophosphinate (6078-99-5) + 2-(diethylphosphinothioyl)-5-chlorobenzothiazole

Guidance literature:

With hydridotetakis(triphenylphosphine)rhodium(I); 1,2-bis[bis(4-methoxyphenyl)phosphanyl]ethane; In tetrahydrofuran; for 3h; Inert atmosphere; Reflux;

DOI:10.1002/adsc.201800630

Reference yield: 99.0%

tetraethyldiphosphine disulfide (3790-23-6) + C19H12ClNOS → 4-chlorophenyl diethyldithiophosphinate (6078-99-5) + 2-(diethylphosphinothioyl)-5-phenylbenzoxazole

Guidance literature:

With hydridotetakis(triphenylphosphine)rhodium(I); 1,2-bis[bis(4-methoxyphenyl)phosphanyl]ethane; In tetrahydrofuran; for 3h; Inert atmosphere; Reflux;

DOI:10.1002/adsc.201800630

upstream raw materials:

4,4'-dichlorodiphenyl disulfide

diethyl(4-(dimethylamino)benzoyl)phosphine sulfide

tetraethyldiphosphine disulfide

2-[(4′-chlorophenyl)thio]benzothiazole