Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2

Base Information

Chemical Name:Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2
CAS No.:149830-13-7
Molecular Formula:C₆₀H₃₈F₈N₄OsS₂
Molecular Weight:1221.31
Hs Code.:

Synonyms:Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2

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Technology Process of Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2

There total 3 articles about Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 65814-72-4
[OsO₂(meso-tetrakis(p-tolyl)porphyrinato)]

: 769-40-4
2,3,5,6-tetrafluorothiophenol

: 149830-13-7
Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2

Guidance literature:: In dichloromethane; byproducts: H2O; 40 min at room temp.; concn. in vac., chromy. (silica, CH2Cl2), recrystn. (CH2Cl2/heptane); elem. anal.;

Reference yield:

: 65748-44-9
Os(TTP)(OCH₃)2

: 149830-13-7
Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: triethylamine / dichloromethane

With triethylamine; In dichloromethane;

Reference yield:

: Os(meso-tetra-p-tolylporphyrinate)(trifluoroacetate)2*CH₂Cl₂

: 769-40-4
2,3,5,6-tetrafluorothiophenol

: 149830-13-7
Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2

Guidance literature:: With triethylamine; In dichloromethane; 3 h at room temp. in the open air; concn. in vac., passed through a silica plug, eluted with CH2Cl2, recrystn. (CH2Cl2/hexane);