Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py)

Base Information

Chemical Name:Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py)
CAS No.:149830-22-8
Molecular Formula:C₅₉H₄₂F₄N₅OsS
Molecular Weight:1119.28
Hs Code.:

Synonyms:Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py)

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Chemical Property of Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py)

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Technology Process of Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py)

There total 5 articles about Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 149830-13-7
Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)2

: 149830-22-8
Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py)

Guidance literature:: With pyridine; In benzene; refluxed for 3 h; cooled, concd. in vac., column chromy. (silica, CH2Cl2), recrystn. (CH2Cl2/hexane); elem. anal.;

Reference yield: 72.0%

: {Os(meso-tetra-p-tolylporphyrinate)}2BF₄

: 769-40-4
2,3,5,6-tetrafluorothiophenol

: 149830-22-8
Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py)

Guidance literature:: With pyridine; In pyridine; stirred for 25 min; stripped to dryness, recrystn. (CH2Cl2/hexane);

Reference yield:

: 65748-44-9
Os(TTP)(OCH₃)2

: 149830-22-8
Os(meso-tetra-p-tolylporphyrinate)(2,3,5,6-tetrafluorothiophenolate)(py)

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane

2: triethylamine / dichloromethane

3: pyridine / benzene

With triethylamine; pyridine; In dichloromethane; benzene;