3-(p-methoxyphenylthio)-5-nitrophthalic anhydride

Base Information

Chemical Name:3-(p-methoxyphenylthio)-5-nitrophthalic anhydride
CAS No.:81116-62-3
Molecular Formula:C₁₅H₉NO₆S
Molecular Weight:331.306
Hs Code.:

Synonyms:3-(p-methoxyphenylthio)-5-nitrophthalic anhydride

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Chemical Property of 3-(p-methoxyphenylthio)-5-nitrophthalic anhydride

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Technology Process of 3-(p-methoxyphenylthio)-5-nitrophthalic anhydride

There total 2 articles about 3-(p-methoxyphenylthio)-5-nitrophthalic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 696-63-9
4-Methoxybenzenethiol

: 52806-20-9
3,5-Dinitrophthalic anhydride

: 81116-62-3
3-(p-methoxyphenylthio)-5-nitrophthalic anhydride

Guidance literature:: With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; acetic anhydride; for 2h;
DOI:10.1002/hlca.19850680405

Reference yield:

: 4277-02-5
3,5-dinitrophthalic acid

: 81116-62-3
3-(p-methoxyphenylthio)-5-nitrophthalic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: Ac₂O / toluene / 1 h / Heating

2: 31 percent / 33 percent KOH, benzyltriethylammonium chloride / acetic anhydride; CH₂Cl₂ / 2 h

With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; acetic anhydride; In dichloromethane; acetic anhydride; toluene;
DOI:10.1002/hlca.19850680405