methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate

Base Information

Chemical Name:methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate
CAS No.:1544664-09-6
Molecular Formula:C₂₀H₂₀F₃IO₃
Molecular Weight:492.277
Hs Code.:

Synonyms:methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate

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Chemical Property of methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate

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Technology Process of methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate

There total 4 articles about methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1544664-07-4
methyl 2-(6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalene-2-yl)acetate

: 1544664-09-6
methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate

Guidance literature:: With N-iodo-succinimide; trifluoroacetic acid; In acetonitrile; at 20 ℃; for 16h;

Reference yield:

: 10441-46-0
6-Hydroxy-2-naphthyl acetic acid

: 1544664-09-6
methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 16 h / Reflux

2: caesium carbonate / 2-methyl-propan-1-ol / 16 h / Reflux

3: sulfuric acid / Reflux

4: N-iodo-succinimide; trifluoroacetic acid / acetonitrile / 16 h / 20 °C

With N-iodo-succinimide; sulfuric acid; caesium carbonate; trifluoroacetic acid; In 2-methyl-propan-1-ol; acetonitrile;

Reference yield:

: 1544665-69-1
C₁₉H₁₉F₃O₃

: 1544664-09-6
methyl 2-(5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)naphthalen-2-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / Reflux

2: N-iodo-succinimide; trifluoroacetic acid / acetonitrile / 16 h / 20 °C

With N-iodo-succinimide; sulfuric acid; trifluoroacetic acid; In acetonitrile;