C₃₀H₃₉N₃O₁₀

Base Information

• Chemical Name: C₃₀H₃₉N₃O₁₀
• CAS No.: 1285486-67-0
• Molecular Formula: C₃₀H₃₉N₃O₁₀
• Molecular Weight: 601.654
• Mol file: 1285486-67-0.mol

Synonyms:C₃₀H₃₉N₃O₁₀

Chemical Property of C₃₀H₃₉N₃O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₉N₃O₁₀

There total 6 articles about C₃₀H₃₉N₃O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3-(3-(2-hydroxyethyl)-5,5-spiroadamantyl-1,2,4-trioxolan-3-yl)-N-(3-(2-oxopyrrolidin-1-yl)propyl)propanamide (1206603-64-6) + 4-Nitrophenyl chloroformate (7693-46-1) → C30H39N3O10 (1285486-67-0)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1002/cmdc.201100002

Reference yield:

OZ-05 (476372-97-1) → C30H39N3O10 (1285486-67-0)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 48 h / 20 °C

2: toluene / 5 h / 50 °C

3: dmap; triethylamine / dichloromethane / 16 h / 20 °C

With dmap; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene; 1: Baeyer-Villiger oxidation;

DOI:10.1002/cmdc.201100002

Reference yield:

adamantan-2-one O-methyloxime (76300-15-7) → C30H39N3O10 (1285486-67-0)

Guidance literature:

Multi-step reaction with 4 steps

1: ozone / dichloromethane; pentane / 1 h / 0 °C

2: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 48 h / 20 °C

3: toluene / 5 h / 50 °C

4: dmap; triethylamine / dichloromethane / 16 h / 20 °C

With dmap; sodium hydrogencarbonate; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene; pentane; 2: Baeyer-Villiger oxidation;

DOI:10.1002/cmdc.201100002

upstream raw materials:

OZ-05

2-Adamantanone

adamantane-2-spiro-3'-9'-oxo-1',2',4',8'-tetraoxaspiro[4.6]undecane

3-(3-(2-hydroxyethyl)-5,5-spiroadamantyl-1,2,4-trioxolan-3-yl)-N-(3-(2-oxopyrrolidin-1-yl)propyl)propanamide

Downstream raw materials:

C₄₆H₆₂F₄N₆O₉