(Z)-ethyl 2-(bromo(m-tolyl)methylene)-4-formylbutanoate

Base Information

• Chemical Name: (Z)-ethyl 2-(bromo(m-tolyl)methylene)-4-formylbutanoate
• CAS No.: 1357567-01-1
• Molecular Formula: C₁₅H₁₇BrO₃
• Molecular Weight: 325.202
• Mol file: 1357567-01-1.mol

Synonyms:(Z)-ethyl 2-(bromo(m-tolyl)methylene)-4-formylbutanoate

Chemical Property of (Z)-ethyl 2-(bromo(m-tolyl)methylene)-4-formylbutanoate

Chemical Property:

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Technology Process of (Z)-ethyl 2-(bromo(m-tolyl)methylene)-4-formylbutanoate

There total 1 articles about (Z)-ethyl 2-(bromo(m-tolyl)methylene)-4-formylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

ethyl 3-(m-tolyl)propiolate (58686-70-7) + allyl alcohol (107-18-6) → (Z)-ethyl 2-(bromo(m-tolyl)methylene)-4-formylbutanoate (1357567-01-1)

Guidance literature:

With oxygen; copper(ll) bromide; palladium dichloride; In water; toluene; at 60 ℃; for 28h; under 760.051 Torr; stereoselective reaction;

DOI:10.1021/jo202416h

upstream raw materials:

ethyl 3-(m-tolyl)propiolate

allyl alcohol

Refernces