(S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol tosylate

Base Information

Chemical Name:(S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol tosylate
CAS No.:187084-12-4
Molecular Formula:C₂₀H₂₆O₅S
Molecular Weight:378.489
Hs Code.:

Synonyms:(S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol tosylate

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Chemical Property of (S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol tosylate

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Technology Process of (S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol tosylate

There total 2 articles about (S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 98-59-9
p-toluenesulfonyl chloride

: 187084-11-3
(S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol

: 187084-12-4
(S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol tosylate

Guidance literature:: With pyridine; In chloroform; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(96)01134-9

Reference yield:

: 187083-86-9
(S)-1-benzyloxy-4-(3,5-dimethoxyphenyl)-2-methylbutane

: 187084-12-4
(S)-4-(3,5-dimethoxyphenyl)-2-methyl-1-butanol tosylate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / lithium, liq. NH₃ / diethyl ether / 0.5 h / -78 °C

2: 78 percent / pyridine / CHCl₃ / 18 h / Ambient temperature

With pyridine; ammonia; lithium; In diethyl ether; chloroform;
DOI:10.1016/S0040-4020(96)01134-9