C₃₃H₃₃N₃O₇

Base Information

Chemical Name:C₃₃H₃₃N₃O₇
CAS No.:1300590-73-1
Molecular Formula:C₃₃H₃₃N₃O₇
Molecular Weight:583.641
Hs Code.:

C<sub>33</sub>H<sub>33</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₃₃H₃₃N₃O₇

Suppliers and Price of C₃₃H₃₃N₃O₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₃₃N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₃₃N₃O₇

There total 12 articles about C₃₃H₃₃N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3587-60-8
Benzyloxymethyl chloride

: 1300589-88-1
C₂₅H₂₅N₃O₆

: 1300590-73-1
C₃₃H₃₃N₃O₇

Guidance literature:: C₂₅H₂₅N₃O₆; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; for 0.25h; Inert atmosphere; Cooling with ice;

Benzyloxymethyl chloride; In N,N-dimethyl-formamide; for 0.5h; Cooling with ice;

Reference yield:

: 153186-10-8
((3aR,5R,6S,6aR)-6-(benzyloxy)-5-((benzyloxy)methyl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 1300590-73-1
C₃₃H₃₃N₃O₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: dmap; triethylamine / dichloromethane / 20 h / Inert atmosphere; Cooling; Reflux

2.1: sulfuric acid; acetic acid / 3.5 h

3.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / 20 °C / Inert atmosphere; Reflux

4.1: methylamine / water; tetrahydrofuran / 0.5 h / 20 °C

5.1: dmap; trifluoromethane sulfonyl chloride / dichloromethane / 1 h / 20 °C / Inert atmosphere; Cooling with ice

6.1: sodium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C

7.1: pyridine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

8.1: sodium azide / N,N-dimethyl-formamide / 48 h / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12.5 h / Inert atmosphere

10.1: dipyridinium dichromate / N,N-dimethyl-formamide / 4.5 h / 20 °C / Inert atmosphere; Molecular sieve

10.2: 1 h

11.1: water; tributylphosphine / tetrahydrofuran / 3.5 h / 20 °C

12.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 21.5 h / 20 °C / Inert atmosphere; Cooling with ice

13.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.25 h / Inert atmosphere; Cooling with ice

13.2: 0.5 h / Cooling with ice

With pyridine; dmap; dipyridinium dichromate; sodium azide; N,O-bis-(trimethylsilyl)-acetamide; tributylphosphine; trifluoromethane sulfonyl chloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; tetrabutyl ammonium fluoride; water; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; methylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 3,5-di-O-benzyl-4-C-(tert-butyldiphenylsilyloxymethyl)-1,2-O-isopropylidene-α-D-ribofuranose

: 1300590-73-1
C₃₃H₃₃N₃O₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: sulfuric acid; acetic acid / 3.5 h

2.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / 20 °C / Inert atmosphere; Reflux

3.1: methylamine / water; tetrahydrofuran / 0.5 h / 20 °C

4.1: dmap; trifluoromethane sulfonyl chloride / dichloromethane / 1 h / 20 °C / Inert atmosphere; Cooling with ice

5.1: sodium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C

6.1: pyridine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

7.1: sodium azide / N,N-dimethyl-formamide / 48 h / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12.5 h / Inert atmosphere

9.1: dipyridinium dichromate / N,N-dimethyl-formamide / 4.5 h / 20 °C / Inert atmosphere; Molecular sieve

9.2: 1 h

10.1: water; tributylphosphine / tetrahydrofuran / 3.5 h / 20 °C

11.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 21.5 h / 20 °C / Inert atmosphere; Cooling with ice

12.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.25 h / Inert atmosphere; Cooling with ice

12.2: 0.5 h / Cooling with ice

With pyridine; dmap; dipyridinium dichromate; sodium azide; N,O-bis-(trimethylsilyl)-acetamide; tributylphosphine; trifluoromethane sulfonyl chloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; tetrabutyl ammonium fluoride; water; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; methylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;