(-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

Base Information

Chemical Name:(-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane
CAS No.:1032401-63-0
Molecular Formula:C₂₄H₃₃BrO₂
Molecular Weight:433.429
Hs Code.:

Synonyms:(-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

Suppliers and Price of (-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

There total 2 articles about (-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1032401-55-0
(+)-(1S,3aS,7aS)-1-tert-butoxy-7a-ethyl-3a,6,7,7a-tetrahydroindane

: 213599-26-9
(Z)-2-(2-iodoethenyl)-4-methoxybromobenzol

: 1032401-63-0
(-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

: 1032401-65-2
(-)-(1S,3aS,4S,7aS)-4(E)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

Guidance literature:: With silver carbonate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 95 ℃; for 5.33333h;

Reference yield:

: 1032401-60-7
(-)-(1S,5S,7aS)-1-tert-butoxy-7a-ethyl-7,7a-dihydroindan-5-yl-formate

: 213599-26-9
(Z)-2-(2-iodoethenyl)-4-methoxybromobenzol

: C₂₄H₃₃BrO₂

: 1032401-63-0
(-)-(1S,3aS,4S,7aS)-4-(Z)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

: 1032401-65-2
(-)-(1S,3aS,4S,7aS)-4(E)-(2-bromo-5-methoxystyryl)-1-tert-butoxy-7a-ethyl-3a,4,7,7a-tetrahydroindane

Guidance literature:: (-)-(1S,5S,7aS)-1-tert-butoxy-7a-ethyl-7,7a-dihydroindan-5-yl-formate; With tributylphosphine; palladium diacetate; In 1,4-dioxane; at 20 - 90 ℃;

(Z)-2-(2-iodoethenyl)-4-methoxybromobenzol; With palladium diacetate; triphenylphosphine; silver carbonate; In N,N-dimethyl-formamide; at 95 ℃;
DOI:10.1002/chem.200700182