Biphenyl-4-carboxylic acid N'-(3-nitro-pyridin-4-yl)-hydrazide; hydrochloride

Base Information

Chemical Name:Biphenyl-4-carboxylic acid N'-(3-nitro-pyridin-4-yl)-hydrazide; hydrochloride
CAS No.:121845-72-5
Molecular Formula:C₁₈H₁₄N₄O₃*ClH
Molecular Weight:370.795
Hs Code.:

Synonyms:Biphenyl-4-carboxylic acid N'-(3-nitro-pyridin-4-yl)-hydrazide; hydrochloride

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Chemical Property of Biphenyl-4-carboxylic acid N'-(3-nitro-pyridin-4-yl)-hydrazide; hydrochloride

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Biphenyl-4-carboxylic acid N'-(3-nitro-pyridin-4-yl)-hydrazide; hydrochloride

There total 3 articles about Biphenyl-4-carboxylic acid N'-(3-nitro-pyridin-4-yl)-hydrazide; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 121845-72-5
Biphenyl-4-carboxylic acid N'-(3-nitro-pyridin-4-yl)-hydrazide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / PCl₅, POCl₃ / 6 h / 130 - 140 °C

2: 12.5 g / ethanol / 5 h / Heating

With phosphorus pentachloride; trichlorophosphate; In ethanol;
DOI:10.1021/jm00131a010

Reference yield:

: 626-64-2,157061-69-3
pyridin-4-ol

: 121845-72-5
Biphenyl-4-carboxylic acid N'-(3-nitro-pyridin-4-yl)-hydrazide; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / HNO₃, H₂SO₄, SO₃ / 1 h / Heating

2: 87 percent / PCl₅, POCl₃ / 6 h / 130 - 140 °C

3: 12.5 g / ethanol / 5 h / Heating

With phosphorus pentachloride; sulfuric acid; sulfur trioxide; nitric acid; trichlorophosphate; In ethanol;
DOI:10.1021/jm00131a010