5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide

Base Information

Chemical Name:5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide
CAS No.:1414967-58-0
Molecular Formula:C₂₁H₂₅N₃O₅S
Molecular Weight:431.513
Hs Code.:

Synonyms:5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide

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Chemical Property of 5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide

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Technology Process of 5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide

There total 4 articles about 5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 1414968-20-9
[1-(5-Phenethylcarbamoyl-furan-2-sulfonyl)-piperidin-4-yl]-carbamic acid tert-butyl ester

: 814-68-6,25189-84-8
acryloyl chloride

: 1414967-58-0
5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide

Guidance literature:: [1-(5-Phenethylcarbamoyl-furan-2-sulfonyl)-piperidin-4-yl]-carbamic acid tert-butyl ester; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

acryloyl chloride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 73874-95-0
(piperidin-4-yl)carbamic acid tert-butyl ester

: 1414967-58-0
5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: methanol / 20 - 45 °C

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

3.2: 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 69816-05-3
2-furancarboxylic acid 5-(chlorosulfonyl) methyl ester

: 1414967-58-0
5-(4-Acryloylamino-piperidine-1-sulfonyl)-furan-2-carboxylic acid phenethyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: methanol / 20 - 45 °C

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

3.2: 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; dichloromethane;