1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene

Base Information

Chemical Name:1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene
CAS No.:865179-31-3
Molecular Formula:C₃₀H₂₀BrNO₂S₄
Molecular Weight:634.662
Hs Code.:

Synonyms:1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene

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Chemical Property of 1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene

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Technology Process of 1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene

There total 8 articles about 1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 865179-30-2
C₂₄H₁₆INO₂S₃

: 106-53-6
para-bromobenzenethiol

: 865179-31-3
1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; potassium tert-butylate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; at 50 ℃; for 24h;
DOI:10.1016/j.tetlet.2005.06.143

Reference yield:

: 865179-25-5
1-(4-nitrophenylthio)-4-(4-bromophenylthio)benzene

: 865179-31-3
1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / CuI; INa; racemic trans-N,N'-dimethyl-1,2-cyclohexanediamine / dioxane / 48 h / 140 °C

2: 76 percent / KOtBu; dppf; Pd(dba)2 / toluene / 24 h / 50 °C

3: 71 percent / CuI; INa; racemic trans-N,N'-dimethyl-1,2-cyclohexanediamine / dioxane / 48 h / 140 °C

4: 69 percent / KOtBu; dppf; Pd(dba)2 / toluene / 24 h / 50 °C

With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; 1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; potassium tert-butylate; sodium iodide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; toluene;
DOI:10.1016/j.tetlet.2005.06.143

Reference yield:

: 865179-27-7
I(C₆H₄S-4)2C₆H₄NO₂-4

: 865179-31-3
1-(4-nitrophenylthio)phenylthio-4-(4-bromophenylthio)phenylthio-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / KOtBu; dppf; Pd(dba)2 / toluene / 24 h / 50 °C

2: 71 percent / CuI; INa; racemic trans-N,N'-dimethyl-1,2-cyclohexanediamine / dioxane / 48 h / 140 °C

3: 69 percent / KOtBu; dppf; Pd(dba)2 / toluene / 24 h / 50 °C

With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; 1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; potassium tert-butylate; sodium iodide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; toluene;
DOI:10.1016/j.tetlet.2005.06.143