5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Name:5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide
CAS No.:955084-10-3
Molecular Formula:C₁₆H₁₃BF₂N₂
Molecular Weight:282.1
Hs Code.:

Synonyms:5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Property of 5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

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Technology Process of 5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

There total 7 articles about 5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 8-(methylthio)-4,4,difluoro-4-bora-3a,4a-diaza-s-indacene

: 5720-05-8
4-methylphenylboronic acid

: 955084-10-3
5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane; In tetrahydrofuran; for 1.5h; Schlenk technique; Inert atmosphere; Heating;
DOI:10.1021/acs.joc.5b00731

Reference yield: 84.0%

: 109-63-7
boron trifluoride diethyl etherate

: 147804-55-5
5-(4-methylphenyl)dipyrromethane

: 955084-10-3
5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: 5-(4-methylphenyl)dipyrromethane; With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 25 ℃; Inert atmosphere;

With triethylamine; In dichloromethane; at 25 ℃; for 0.25h; Inert atmosphere;

boron trifluoride diethyl etherate; In dichloromethane; at 25 ℃; Inert atmosphere;
DOI:10.1039/c6ra12258b

Reference yield: 77.0%

: 8-(methylthio)-4,4,difluoro-4-bora-3a,4a-diaza-s-indacene

: 31614-66-1
tributyl(p-tolyl)stannane

: 955084-10-3
5,5-difluoro-10-(p-tolyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ((diphenylphosphoryl)oxy)copper(I); In tetrahydrofuran; for 0.5h; Reagent/catalyst; Schlenk technique; Inert atmosphere; Heating;
DOI:10.1021/acs.joc.5b00731