Technology Process of 7H-Pyrrolo(3,2,1-de)phenanthridin-7-one, 10-hydroxy-9-methoxy-
There total 8 articles about 7H-Pyrrolo(3,2,1-de)phenanthridin-7-one, 10-hydroxy-9-methoxy- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
aluminum (III) chloride;
In
dichloromethane;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/acs.orglett.0c01082
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 0.89 g / diethyl ether
2: H2 / 10percent Pd-C / ethanol / 4 h / Heating
3: 7 mg / NaNO2, H2SO4 / acetic acid; H2O / 4 h / 100 °C
4: DDQ / benzene / 10 h / Heating
5: piperidine / H2O / 15 h / Heating
With
piperidine; sulfuric acid; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium nitrite;
palladium on activated charcoal;
In
diethyl ether; ethanol; water; acetic acid; benzene;
DOI:10.1016/S0031-9422(00)80167-3
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 0.89 g / diethyl ether
2: H2 / 10percent Pd-C / ethanol / 4 h / Heating
3: 7 mg / NaNO2, H2SO4 / acetic acid; H2O / 4 h / 100 °C
4: DDQ / benzene / 10 h / Heating
5: piperidine / H2O / 15 h / Heating
With
piperidine; sulfuric acid; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium nitrite;
palladium on activated charcoal;
In
diethyl ether; ethanol; water; acetic acid; benzene;
DOI:10.1016/S0031-9422(00)80167-3