5-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-4-hydroxy-pyridazin-3-one

Base Information

Chemical Name:5-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-4-hydroxy-pyridazin-3-one
CAS No.:1443275-00-0
Molecular Formula:C₁₁H₅Cl₂F₃N₂O₂
Molecular Weight:325.074
Hs Code.:

Synonyms:5-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-4-hydroxy-pyridazin-3-one

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Chemical Property of 5-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-4-hydroxy-pyridazin-3-one

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Technology Process of 5-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-4-hydroxy-pyridazin-3-one

There total 2 articles about 5-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-4-hydroxy-pyridazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110386-45-3
4,5-dichloro-2-[2-chloro-4-(trifluoromethyl)phenyl]pyridazin-3-one

: 124-41-4
sodium methylate

: 1443275-00-0
5-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-4-hydroxy-pyridazin-3-one

: 4-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-5-hydroxy-pyridazin-3-one

Guidance literature:: 4,5-dichloro-2-[2-chloro-4-(trifluoromethyl)phenyl]pyridazin-3-one; sodium methylate; With morpholine; In 1,4-dioxane; methanol; at 20 ℃; for 1.08333h; Inert atmosphere;

With morpholine; at 100 ℃; for 3h; Inert atmosphere;

Reference yield:

: 86398-98-3
2-chloro-4-trifluoromethylphenyl hydrazine

: 1443275-00-0
5-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-4-hydroxy-pyridazin-3-one

: 4-chloro-2-[2-chloro-4-(trifluoromethyl)phenyl]-5-hydroxy-pyridazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / 25 - 140 °C / Microwave irradiation

2.1: morpholine / 1,4-dioxane; methanol / 1.08 h / 20 °C / Inert atmosphere

2.2: 3 h / 100 °C / Inert atmosphere

With morpholine; hydrogenchloride; In 1,4-dioxane; methanol; water;