methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate

Base Information

• Chemical Name: methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate
• CAS No.: 243866-35-5
• Molecular Formula: C₁₆H₂₂O₈S
• Molecular Weight: 374.412

Synonyms:methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate

Chemical Property of methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate

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Technology Process of methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate

There total 1 articles about methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

Methyl (phenyl 4,5,7,8,9-penta-O-acetyl-3-deoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate → methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate (243866-35-5)

Guidance literature:

With sodium methylate; In methanol; at 0 ℃; for 2h; pH=9.0;

DOI:10.1080/07328309908544026

Reference yield: 97.0%

trityl chloride (76-83-5) + methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate (243866-35-5) → methyl (phenyl 9-O-triphenylmethyl-3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate (243866-50-4)

Guidance literature:

With pyridine; at 20 ℃; for 17h;

DOI:10.1080/07328309908544026

Reference yield: 92.0%

2,2-dimethoxy-propane (77-76-9) + methyl (phenyl 3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate (243866-35-5) → methyl (phenyl 3-deoxy-8,9-O-isopropylidene-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate (243866-36-6)

Guidance literature:

With Dowex 50W-X₈ (H⁺ form); In acetone; at 20 ℃; for 6h;

DOI:10.1080/07328309908544026

Downstream raw materials:

methyl (phenyl 9-O-triphenylmethyl-3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate

methyl (phenyl 9-O-t-butyldimethylsilyl-3-deoxy-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate

methyl (phenyl 3-deoxy-8,9-O-isopropylidene-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate

methyl (phenyl 4,5,7-tri-O-acetyl-3-deoxy-8,9-O-isopropylidene-2-thio-β-D-glycero-D-galacto-2-nonulopyranosid)onate

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