tetraethyl 5,8-dimethyl-6-((trimethylsilyl)oxy)naphthalene-2,2,3,3(1H,4H)-tetracarboxylate

Base Information

• Chemical Name: tetraethyl 5,8-dimethyl-6-((trimethylsilyl)oxy)naphthalene-2,2,3,3(1H,4H)-tetracarboxylate
• CAS No.: 1300749-63-6
• Molecular Formula: C₂₇H₄₀O₉Si
• Molecular Weight: 536.695

Synonyms:tetraethyl 5,8-dimethyl-6-((trimethylsilyl)oxy)naphthalene-2,2,3,3(1H,4H)-tetracarboxylate

Chemical Property of tetraethyl 5,8-dimethyl-6-((trimethylsilyl)oxy)naphthalene-2,2,3,3(1H,4H)-tetracarboxylate

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Technology Process of tetraethyl 5,8-dimethyl-6-((trimethylsilyl)oxy)naphthalene-2,2,3,3(1H,4H)-tetracarboxylate

There total 1 articles about tetraethyl 5,8-dimethyl-6-((trimethylsilyl)oxy)naphthalene-2,2,3,3(1H,4H)-tetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

trimetylsilylketene (4071-85-6) + C23H32O8 → 6-hydroxy-5,8-dimethyl-1,4-dihydronaphthalene-2,2,3,3-tetracarboxylic acid tetraethyl ester (1131477-36-5) + tetraethyl 5,8-dimethyl-6-((trimethylsilyl)oxy)naphthalene-2,2,3,3(1H,4H)-tetracarboxylate (1300749-63-6)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,4-di(diphenylphosphino)-butane; In toluene; at 60 ℃; for 5h; Inert atmosphere;

DOI:10.1021/ja2007627

upstream raw materials:

trimetylsilylketene

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