6-hydroxy-5,8-dimethyl-1,4-dihydronaphthalene-2,2,3,3-tetracarboxylic acid tetraethyl ester

Base Information

• Chemical Name: 6-hydroxy-5,8-dimethyl-1,4-dihydronaphthalene-2,2,3,3-tetracarboxylic acid tetraethyl ester
• CAS No.: 1131477-36-5
• Molecular Formula: C₂₄H₃₂O₉
• Molecular Weight: 464.513

Synonyms:6-hydroxy-5,8-dimethyl-1,4-dihydronaphthalene-2,2,3,3-tetracarboxylic acid tetraethyl ester

Chemical Property of 6-hydroxy-5,8-dimethyl-1,4-dihydronaphthalene-2,2,3,3-tetracarboxylic acid tetraethyl ester

Chemical Property:

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Technology Process of 6-hydroxy-5,8-dimethyl-1,4-dihydronaphthalene-2,2,3,3-tetracarboxylic acid tetraethyl ester

There total 1 articles about 6-hydroxy-5,8-dimethyl-1,4-dihydronaphthalene-2,2,3,3-tetracarboxylic acid tetraethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

trimetylsilylketene (4071-85-6) + C23H32O8 → 6-hydroxy-5,8-dimethyl-1,4-dihydronaphthalene-2,2,3,3-tetracarboxylic acid tetraethyl ester (1131477-36-5) + tetraethyl 5,8-dimethyl-6-((trimethylsilyl)oxy)naphthalene-2,2,3,3(1H,4H)-tetracarboxylate (1300749-63-6)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,4-di(diphenylphosphino)-butane; In toluene; at 60 ℃; for 5h; Inert atmosphere;

DOI:10.1021/ja2007627

upstream raw materials:

trimetylsilylketene

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