5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine

Base Information

Chemical Name:5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine
CAS No.:1365259-03-5
Molecular Formula:C₁₅H₁₅IN₆O
Molecular Weight:422.228
Hs Code.:

Synonyms:5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine

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Chemical Property of 5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine

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Technology Process of 5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine

There total 3 articles about 5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1725-81-1
((3-iodoprop-2-yn-1-yl)oxy)benzene

: 63423-50-7
5‐(azidomethyl)‐2‐methylpyrimidin‐4‐amine

: 1365259-03-5
5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine

Guidance literature:: With copper(l) iodide; triethylamine; In tetrahydrofuran; at 40 - 50 ℃; for 12h;

Reference yield:

: 108-95-2,27073-41-2
phenol

: 1365259-03-5
5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 5 h / Reflux

2: N-iodomorpholine; copper(l) iodide / tetrahydrofuran / 1 h / 20 °C

3: copper(l) iodide; triethylamine / tetrahydrofuran / 12 h / 20 °C

With N-iodomorpholine; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; acetone;
DOI:10.1016/j.bmc.2012.01.019

Reference yield:

: 59-43-8
vitamin B₁

: 1365259-03-5
5-((5-iodo-4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl)methyl)-2-methylpyrimidin-4-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; sodium sulfite / water / 6 h / 60 - 65 °C

2: copper(l) iodide; triethylamine / tetrahydrofuran / 12 h / 20 °C

With copper(l) iodide; sodium azide; triethylamine; sodium sulfite; In tetrahydrofuran; water;
DOI:10.1016/j.bmc.2012.01.019