15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol

Base Information

Chemical Name:15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol
CAS No.:725712-11-8
Molecular Formula:C₃₈H₆₂O₄
Molecular Weight:582.908
Hs Code.:

Synonyms:15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol

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Chemical Property of 15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol

Chemical Property:

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Technology Process of 15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol

There total 3 articles about 15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 18295-60-8
propargyl magnesium bromide

: 725712-09-4
12-[2-(12-oxo-dodecyloxymethyl)-benzyloxy]-dodecanal

: 725712-11-8
15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; at -78 - 20 ℃;
DOI:10.1002/ejoc.200300792

Reference yield:

: 5675-51-4
1,12-dodecandiol

: 725712-11-8
15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / NaH / tetrahydrofuran

2: 80 percent / oxalyl chloride; DMSO / triethylamine

3: 83 percent / DIBAH / diethyl ether / -78 - 20 °C

With oxalyl dichloride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; triethylamine; 2: Swern oxidation;
DOI:10.1002/ejoc.200300792

Reference yield:

: 725712-05-0
12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecan-1-ol

: 725712-11-8
15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / oxalyl chloride; DMSO / triethylamine

2: 83 percent / DIBAH / diethyl ether / -78 - 20 °C

With oxalyl dichloride; diisobutylaluminium hydride; dimethyl sulfoxide; In diethyl ether; triethylamine; 1: Swern oxidation;
DOI:10.1002/ejoc.200300792