15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one

Base Information

Chemical Name:15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one
CAS No.:725712-13-0
Molecular Formula:C₃₈H₅₈O₄
Molecular Weight:578.876
Hs Code.:

Synonyms:15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one

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Chemical Property of 15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one

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Technology Process of 15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one

There total 4 articles about 15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 725712-11-8
15-[2-(12-hydroxy-pentadec-14-ynyloxymethyl)-benzyloxy]-pentadec-1-yn-4-ol

: 725712-13-0
15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃;
DOI:10.1002/ejoc.200300792

Reference yield:

: 5675-51-4
1,12-dodecandiol

: 725712-13-0
15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: 37 percent / NaH / tetrahydrofuran

2: 80 percent / oxalyl chloride; DMSO / triethylamine

3: 83 percent / DIBAH / diethyl ether / -78 - 20 °C

4: 83 percent / Dess-Martin periodine / CH₂Cl₂ / 20 °C

With oxalyl dichloride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; dichloromethane; triethylamine; 2: Swern oxidation;
DOI:10.1002/ejoc.200300792

Reference yield:

: 725712-05-0
12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecan-1-ol

: 725712-13-0
15-[2-(12-oxo-pentadeca-13,14-dienyloxymethyl)-benzyloxy]-pentadeca-1,2-dien-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / oxalyl chloride; DMSO / triethylamine

2: 83 percent / DIBAH / diethyl ether / -78 - 20 °C

3: 83 percent / Dess-Martin periodine / CH₂Cl₂ / 20 °C

With oxalyl dichloride; diisobutylaluminium hydride; Dess-Martin periodane; dimethyl sulfoxide; In diethyl ether; dichloromethane; triethylamine; 1: Swern oxidation;
DOI:10.1002/ejoc.200300792