N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide

Base Information

Chemical Name:N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide
CAS No.:464885-23-2
Molecular Formula:C₅₈H₄₂Br₄N₂O₄
Molecular Weight:1150.6
Hs Code.:

Synonyms:N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide

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Chemical Property of N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide

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Technology Process of N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide

There total 4 articles about N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 187536-95-4
N,N’-bis(2,6-diisopropylphenyl)-terrylene-3,4,11,12-tetracarboximide

: 464885-23-2
N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide

Guidance literature:: With bromine; In chloroform; at 50 ℃; for 12h;
DOI:10.1002/ejoc.201901085

Reference yield: 78.0%

: 464885-23-2
N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide

Guidance literature:

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 464885-23-2
N,N’-di(2,6-diisopropylphenyl)-1,6,9,13-tetrabromoterrylene-3,4:11,12-tetracarboxdiimide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 5 h / 110 °C / Inert atmosphere

2: sodium t-butanolate; DBN / diethylene glycol dimethyl ether / 3 h / 130 °C / Schlenk technique; Inert atmosphere

3: bromine / chloroform / 12 h / 50 °C

With DBN; bromine; acetic acid; sodium t-butanolate; In chloroform; diethylene glycol dimethyl ether;
DOI:10.1002/ejoc.201901085