p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside

Base Information

• Chemical Name: p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside
• CAS No.: 84564-19-2
• Molecular Formula: C₄₇H₄₀N₂O₁₀
• Molecular Weight: 792.842

Synonyms:p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside

Chemical Property of p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside

Chemical Property:

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Technology Process of p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside

There total 4 articles about p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trityl chloride (76-83-5) → p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside (84564-19-2)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / Ambient temperature

2: pyridine / 2 h

In pyridine;

DOI:10.1016/0008-6215(82)85025-8

Reference yield:

4-nitrophenyl N-acetyl-β-D-glucosaminide (3459-18-5,50645-66-4) → p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside (84564-19-2)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / Ambient temperature

2: pyridine / 2 h

In pyridine;

DOI:10.1016/0008-6215(82)85025-8

Reference yield:

benzoyl chloride (98-88-4) + N-[(2S,3R,4R,5S,6R)-4,5-Dihydroxy-2-(4-nitro-phenoxy)-6-trityloxymethyl-tetrahydro-pyran-3-yl]-acetamide → p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside (84564-19-2)

Guidance literature:

In pyridine; for 2h; Yield given;

DOI:10.1016/0008-6215(82)85025-8

upstream raw materials:

benzoyl chloride

trityl chloride

4-nitrophenyl N-acetyl-β-D-glucosaminide

Downstream raw materials:

p-nitrophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

p-trifluoroacetamidophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-6-O-trityl-β-D-glucopyranoside

p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-6-O-α-D-glucopyranosyl-β-D-glucopyranoside

p-trifluoroacetamidophenyl 2-acetamido-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

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