3-amino-2-benzoyl-4-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbamoyl)-5-phenylaminothiophene

Base Information

Chemical Name:3-amino-2-benzoyl-4-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbamoyl)-5-phenylaminothiophene
CAS No.:1269841-08-8
Molecular Formula:C₂₇H₂₂N₄O₂S₂
Molecular Weight:498.629
Hs Code.:

Synonyms:3-amino-2-benzoyl-4-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbamoyl)-5-phenylaminothiophene

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Chemical Property of 3-amino-2-benzoyl-4-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbamoyl)-5-phenylaminothiophene

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Technology Process of 3-amino-2-benzoyl-4-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbamoyl)-5-phenylaminothiophene

There total 2 articles about 3-amino-2-benzoyl-4-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbamoyl)-5-phenylaminothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 73227-84-6
2-cyano-N-(3-cyano-4,5,6,7-tetrahydrobenzo [b]thiophen-2-yl)acetamide

: 103-72-0
phenyl isothiocyanate

: 70-11-1
α-bromoacetophenone

: 1269841-08-8
3-amino-2-benzoyl-4-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbamoyl)-5-phenylaminothiophene

Guidance literature:: 2-cyano-N-(3-cyano-4,5,6,7-tetrahydrobenzo [b]thiophen-2-yl)acetamide; phenyl isothiocyanate; With potassium hydroxide; In N,N-dimethyl-formamide;

α-bromoacetophenone; In N,N-dimethyl-formamide;
DOI:10.3390/molecules16010052

Reference yield:

: 4651-91-6
3-cyano-2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene

: 1269841-08-8
3-amino-2-benzoyl-4-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbamoyl)-5-phenylaminothiophene

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 5 h / Reflux

2: potassium hydroxide / N,N-dimethyl-formamide

With potassium hydroxide; In N,N-dimethyl-formamide;
DOI:10.3390/molecules16010052