C₄₈H₅₆F₃N₃O₈Si

Base Information

Chemical Name:C₄₈H₅₆F₃N₃O₈Si
CAS No.:1359025-20-9
Molecular Formula:C₄₈H₅₆F₃N₃O₈Si
Molecular Weight:888.069
Hs Code.:

C<sub>48</sub>H<sub>56</sub>F<sub>3</sub>N<sub>3</sub>O<sub>8</sub>Si

Synonyms:C₄₈H₅₆F₃N₃O₈Si

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Chemical Property of C₄₈H₅₆F₃N₃O₈Si

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Technology Process of C₄₈H₅₆F₃N₃O₈Si

There total 17 articles about C₄₈H₅₆F₃N₃O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1359025-19-6
C₄₇H₅₄F₃N₃O₈Si

: 1359025-20-9
C₄₈H₅₆F₃N₃O₈Si

Guidance literature:: With water; sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; for 2h;

Reference yield:

: 710-18-9
1-methoxy-4-(trifluoromethoxy)benzene

: 1359025-20-9
C₄₈H₅₆F₃N₃O₈Si

Guidance literature:: Multi-step reaction with 17 steps

1.1: sulfuric acid; nitric acid / dichloromethane / 0 - 20 °C

2.1: sodium dithionite; water / tetrahydrofuran / 16 h / 20 °C

3.1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 0 °C

4.1: hydrogenchloride; sodium nitrite / 1,4-dioxane; water / 0.5 h / 20 °C

4.2: 72 h / 0 - 20 °C

5.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / -78 °C

5.2: 2 h / -78 - 20 °C

6.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 0 - 20 °C

7.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 20 °C

8.1: n-butyllithium; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; triethylamine hydrochloride / tetrahydrofuran; hexane / 1 h / -78 °C

8.2: 2.02 h / -78 - 20 °C

9.1: boron tribromide / dichloromethane / 1 h / -78 - 0 °C

9.2: 0.25 h / 20 °C

10.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

11.1: n-butyllithium / tetrahydrofuran / 0.33 h / -100 °C / Inert atmosphere

11.2: 1.08 h / -100 - -78 °C

12.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

13.1: sodium tetrahydroborate / 1,2-dichloro-ethane / 2 h / 20 °C

14.1: potassium carbonate / acetonitrile / 2 h / 30 °C

15.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexane / 0.17 h / -78 °C

15.2: 1 h / -78 - 0 °C

16.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 24 h / 35 °C / Inert atmosphere

17.1: water; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 2 h

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; sodium dithionite; oxalyl dichloride; 1,3-dimethylbarbituric acid; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; water; isopropylmagnesium chloride; nitric acid; boron tribromide; triethylamine hydrochloride; sodium tris(acetoxy)borohydride; potassium carbonate; pyridinium hydrobromide perbromide; diisopropylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; sodium nitrite; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 660848-57-7
2-methoxy-5-(trifluoromethoxy)aniline

: 1359025-20-9
C₄₈H₅₆F₃N₃O₈Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 0 °C

2.1: hydrogenchloride; sodium nitrite / 1,4-dioxane; water / 0.5 h / 20 °C

2.2: 72 h / 0 - 20 °C

3.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / -78 °C

3.2: 2 h / -78 - 20 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 0 - 20 °C

5.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 20 °C

6.1: n-butyllithium; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; triethylamine hydrochloride / tetrahydrofuran; hexane / 1 h / -78 °C

6.2: 2.02 h / -78 - 20 °C

7.1: boron tribromide / dichloromethane / 1 h / -78 - 0 °C

7.2: 0.25 h / 20 °C

8.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

9.1: n-butyllithium / tetrahydrofuran / 0.33 h / -100 °C / Inert atmosphere

9.2: 1.08 h / -100 - -78 °C

10.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

11.1: sodium tetrahydroborate / 1,2-dichloro-ethane / 2 h / 20 °C

12.1: potassium carbonate / acetonitrile / 2 h / 30 °C

13.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexane / 0.17 h / -78 °C

13.2: 1 h / -78 - 0 °C

14.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 24 h / 35 °C / Inert atmosphere

15.1: water; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 2 h

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; 1,3-dimethylbarbituric acid; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; water; isopropylmagnesium chloride; boron tribromide; triethylamine hydrochloride; sodium tris(acetoxy)borohydride; potassium carbonate; pyridinium hydrobromide perbromide; diisopropylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; sodium nitrite; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;