N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine

Base Information

Chemical Name:N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine
CAS No.:1452392-79-8
Molecular Formula:C₁₅H₁₇N₃O
Molecular Weight:255.319
Hs Code.:

Synonyms:N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine

Chemical Property:

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Technology Process of N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine

There total 4 articles about N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10472-24-9,265317-94-0
methyl 2-oxocyclopentane-1-carboxylate

: 1452392-79-8
N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium formate / methanol / 24 h / Reflux

2: acetic anhydride / 4 h / 20 °C / Cooling with ice

3: ammonium formate; formamide / 16 h / 20 - 150 °C

4: trichlorophosphate / 3 h / Reflux

5: hydrogenchloride / isopropyl alcohol / Reflux

With hydrogenchloride; ammonium formate; acetic anhydride; formamide; trichlorophosphate; In methanol; isopropyl alcohol;
DOI:10.1021/jm400639z

Reference yield:

: 52909-60-1
2aminocyclopentene-1-carboxylic acid methyl ester

: 1452392-79-8
N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine

Guidance literature:: Multi-step reaction with 4 steps

1: acetic anhydride / 4 h / 20 °C / Cooling with ice

2: ammonium formate; formamide / 16 h / 20 - 150 °C

3: trichlorophosphate / 3 h / Reflux

4: hydrogenchloride / isopropyl alcohol / Reflux

With hydrogenchloride; ammonium formate; acetic anhydride; formamide; trichlorophosphate; In isopropyl alcohol;
DOI:10.1021/jm400639z

Reference yield:

: 5661-01-8
6,7-dihydro-3H-cyclopenta[d]pyrimidin-4(5H)-one

: 1452392-79-8
N-(4-methoxyphenyl)-N-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 3 h / Reflux

2: hydrogenchloride / isopropyl alcohol / Reflux

With hydrogenchloride; trichlorophosphate; In isopropyl alcohol;
DOI:10.1021/jm400639z