triphenylphosphine gold N²-[(benzyloxy)carbonyl]-N¹-[(trifluoromethyl)sulfonyl]-(L)-leucinamide

Base Information

• Chemical Name: triphenylphosphine gold N²-[(benzyloxy)carbonyl]-N¹-[(trifluoromethyl)sulfonyl]-(L)-leucinamide
• CAS No.: 1401094-59-4
• Molecular Formula: C₃₃H₃₃AuF₃N₂O₅PS
• Molecular Weight: 854.637

Synonyms:triphenylphosphine gold N²-[(benzyloxy)carbonyl]-N¹-[(trifluoromethyl)sulfonyl]-(L)-leucinamide

Chemical Property of triphenylphosphine gold N²-[(benzyloxy)carbonyl]-N¹-[(trifluoromethyl)sulfonyl]-(L)-leucinamide

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Technology Process of triphenylphosphine gold N²-[(benzyloxy)carbonyl]-N¹-[(trifluoromethyl)sulfonyl]-(L)-leucinamide

There total 4 articles about triphenylphosphine gold N²-[(benzyloxy)carbonyl]-N¹-[(trifluoromethyl)sulfonyl]-(L)-leucinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(triphenylphosphine)gold(I) chloride (14243-64-2) + N2-[(benzyloxy)carbonyl]-N1-[(trifluoromethyl)sulfonyl]-(L)-leucinamide (1401094-69-6) → triphenylphosphine gold N2-[(benzyloxy)carbonyl]-N1-[(trifluoromethyl)sulfonyl]-(L)-leucinamide (1401094-59-4)

Guidance literature:

N²-[(benzyloxy)carbonyl]-N¹-[(trifluoromethyl)sulfonyl]-(L)-leucinamide; With silver carbonate; at 0 ℃; for 0.0833333h;

(triphenylphosphine)gold(I) chloride; In dichloromethane; at 0 ℃; for 48h;

Reference yield:

L-leucine (61-90-5,21675-61-6,25248-98-0,70-45-1) → triphenylphosphine gold N2-[(benzyloxy)carbonyl]-N1-[(trifluoromethyl)sulfonyl]-(L)-leucinamide (1401094-59-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydroxide / water / 2.25 h / 0 - 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxybenzotriazol-hydrate / dichloromethane / 72 h / 0 - 20 °C

3.1: silver carbonate / 0.08 h / 0 °C

3.2: 48 h / 0 °C

With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; silver carbonate; sodium hydroxide; In dichloromethane; water;

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → triphenylphosphine gold N2-[(benzyloxy)carbonyl]-N1-[(trifluoromethyl)sulfonyl]-(L)-leucinamide (1401094-59-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydroxide / water / 2.25 h / 0 - 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxybenzotriazol-hydrate / dichloromethane / 72 h / 0 - 20 °C

3.1: silver carbonate / 0.08 h / 0 °C

3.2: 48 h / 0 °C

With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; silver carbonate; sodium hydroxide; In dichloromethane; water;

upstream raw materials:

L-leucine

benzyl chloroformate

Z-Leu-OH

(triphenylphosphine)gold(I) chloride

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