(2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol

Base Information

Chemical Name:(2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol
CAS No.:81975-96-4
Molecular Formula:C₂₆H₂₈N₂O₃
Molecular Weight:416.52
Hs Code.:

Synonyms:(2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol

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Chemical Property of (2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol

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Technology Process of (2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol

There total 4 articles about (2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 81975-95-3
(+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol

: 81975-96-4
(2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol

Guidance literature:: With sodium hydroxide; In methanol; water;

Reference yield:

: 4148-59-8,29776-38-3
<1,3:2,4>-di-O-benzylideneerythritol

: 81975-96-4
(2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 1 h / 76 °C

2: 67 percent / sodium cyanide / dimethylsulfoxide

3: 70 percent / sodium hypophosphite / Raney nickel / aq. acetic acid; pyridine

4: 93 percent / sodium hydroxide / methanol; H₂O

With sodium cyanide; sodium hydroxide; N-Bromosuccinimide; sodium hypophosphite; Perbenzoic acid; nickel; In pyridine; methanol; tetrachloromethane; water; acetic acid; dimethyl sulfoxide;

Reference yield:

: 81975-93-1,104311-83-3
3-O-benzoyl-2,4-O-benzylidene-1-bromo-1-deoxy-DL-erythritol

: 81975-96-4
(2S,4R,5S)-4-(1,3-Diphenyl-imidazolidin-2-ylmethyl)-2-phenyl-[1,3]dioxan-5-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / sodium cyanide / dimethylsulfoxide

2: 70 percent / sodium hypophosphite / Raney nickel / aq. acetic acid; pyridine

3: 93 percent / sodium hydroxide / methanol; H₂O

With sodium cyanide; sodium hydroxide; sodium hypophosphite; nickel; In pyridine; methanol; water; acetic acid; dimethyl sulfoxide;