(+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol

Base Information

Chemical Name:(+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol
CAS No.:81975-95-3
Molecular Formula:C₃₃H₃₂N₂O₄
Molecular Weight:520.628
Hs Code.:

Synonyms:(+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol

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Chemical Property of (+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol

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Technology Process of (+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol

There total 4 articles about (+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 81975-94-2
4-O-benzoyl-3,5-O-benzylidene-2-deoxy-DL-erythropentanonitrile

: 150-61-8
N,N'-diphenylethylenediamine

: 81975-95-3
(+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol

Guidance literature:: With sodium hypophosphite; nickel; In pyridine; acetic acid;

Reference yield:

: 4148-59-8,29776-38-3
<1,3:2,4>-di-O-benzylideneerythritol

: 81975-95-3
(+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 1 h / 76 °C

2: 67 percent / sodium cyanide / dimethylsulfoxide

3: 70 percent / sodium hypophosphite / Raney nickel / aq. acetic acid; pyridine

With sodium cyanide; N-Bromosuccinimide; sodium hypophosphite; Perbenzoic acid; nickel; In pyridine; tetrachloromethane; acetic acid; dimethyl sulfoxide;

Reference yield:

: 81975-93-1,104311-83-3
3-O-benzoyl-2,4-O-benzylidene-1-bromo-1-deoxy-DL-erythritol

: 81975-95-3
(+/-)-3-O-benzoyl-2,4-O-benzylidene-1-deoxy-1-(1,3-diphenyl-2-imidazolidyl)erythritol

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / sodium cyanide / dimethylsulfoxide

2: 70 percent / sodium hypophosphite / Raney nickel / aq. acetic acid; pyridine

With sodium cyanide; sodium hypophosphite; nickel; In pyridine; acetic acid; dimethyl sulfoxide;