β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate

Base Information

Chemical Name:β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate
CAS No.:297145-20-1
Molecular Formula:C₂₅H₂₉N₃O₁₄
Molecular Weight:595.517
Hs Code.:

Synonyms:β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate

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Chemical Property of β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate

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Technology Process of β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate

There total 6 articles about β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 297145-19-8
dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate

: 297145-20-1
β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate

Guidance literature:: With lithium hydroxide; In water; acetone; at 20 ℃; for 24h;
DOI:10.1139/v99-246

Reference yield:

: 120230-67-3
dimethyl N-(9-phenylfluorenyl)-β,β-dimethyl-(S)-aspartate

: 297145-20-1
β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 10 percent Pd/C / methanol / 24 h / 2585.74 Torr

2: NaHCO₃ / dioxane; H₂O / 16 h / 20 °C

3: LiOH / acetone; H₂O / 48 h / 40 °C

4: CsF / dimethylformamide / 48 h / 20 °C

5: 60 percent / LiOH / acetone; H₂O / 24 h / 20 °C

With lithium hydroxide; hydrogen; sodium hydrogencarbonate; cesium fluoride; palladium on activated charcoal; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; acetone; 1: Hydrogenolysis / 2: Acylation / 3: Hydrolysis / 4: Alkylation / 5: Hydrolysis;
DOI:10.1139/v99-246

Reference yield:

: 42855-00-5
nitroveratryloxycarbonyl chloride

: 297145-20-1
β-nitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-(S)-aspartate

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / dioxane; H₂O / 16 h / 20 °C

2: LiOH / acetone; H₂O / 48 h / 40 °C

3: CsF / dimethylformamide / 48 h / 20 °C

4: 60 percent / LiOH / acetone; H₂O / 24 h / 20 °C

With lithium hydroxide; sodium hydrogencarbonate; cesium fluoride; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetone; 1: Acylation / 2: Hydrolysis / 3: Alkylation / 4: Hydrolysis;
DOI:10.1139/v99-246