dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate

Base Information

Chemical Name:dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate
CAS No.:297145-19-8
Molecular Formula:C₃₄H₃₈N₄O₁₈
Molecular Weight:790.692
Hs Code.:

Synonyms:dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate

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Chemical Property of dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate

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Technology Process of dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate

There total 5 articles about dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120230-67-3
dimethyl N-(9-phenylfluorenyl)-β,β-dimethyl-(S)-aspartate

: 297145-19-8
dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10 percent Pd/C / methanol / 24 h / 2585.74 Torr

2: NaHCO₃ / dioxane; H₂O / 16 h / 20 °C

3: LiOH / acetone; H₂O / 48 h / 40 °C

4: CsF / dimethylformamide / 48 h / 20 °C

With lithium hydroxide; hydrogen; sodium hydrogencarbonate; cesium fluoride; palladium on activated charcoal; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; acetone; 1: Hydrogenolysis / 2: Acylation / 3: Hydrolysis / 4: Alkylation;
DOI:10.1139/v99-246

Reference yield:

: 53413-67-5
6-nitroveratrylbromide

: (S)-3-(4,5-Dimethoxy-2-nitro-benzyloxycarbonylamino)-2,2-dimethyl-succinic acid

: 297145-19-8
dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1139/v99-246

Reference yield:

: 42855-00-5
nitroveratryloxycarbonyl chloride

: 297145-19-8
dinitroveratryl N-(6-nitroveratryloxycarbonyl)-β,β-dimethyl-S-aspartate

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃ / dioxane; H₂O / 16 h / 20 °C

2: LiOH / acetone; H₂O / 48 h / 40 °C

3: CsF / dimethylformamide / 48 h / 20 °C

With lithium hydroxide; sodium hydrogencarbonate; cesium fluoride; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetone; 1: Acylation / 2: Hydrolysis / 3: Alkylation;
DOI:10.1139/v99-246