Technology Process of 3-(4-benzyl-1H-1,2,3-triazol-4-yl)-1H-pyrrolo[2,3-b]pyridine
There total 4 articles about 3-(4-benzyl-1H-1,2,3-triazol-4-yl)-1H-pyrrolo[2,3-b]pyridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 1h;
DOI:10.1039/c1ob05586k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: iodine; potassium hydroxide / N,N-dimethyl-formamide / 20 °C
2: dmap / dichloromethane / 1 h / 20 °C
3: copper(l) iodide; sodium azide; sodium ascorbate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane / water; dimethyl sulfoxide / 112 h / 20 °C / Inert atmosphere
4: potassium carbonate / methanol / 1 h / 20 °C
With
dmap; copper(l) iodide; sodium azide; sodium ascorbate; iodine; potassium carbonate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; potassium hydroxide;
In
methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05586k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; sodium azide; sodium ascorbate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane / water; dimethyl sulfoxide / 112 h / 20 °C / Inert atmosphere
2: potassium carbonate / methanol / 1 h / 20 °C
With
copper(l) iodide; sodium azide; sodium ascorbate; potassium carbonate; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane;
In
methanol; water; dimethyl sulfoxide;
DOI:10.1039/c1ob05586k
