diphenyloctylgermane

Base Information

Chemical Name:diphenyloctylgermane
CAS No.:100184-63-2
Molecular Formula:C₂₀H₂₈Ge
Molecular Weight:341.032
Hs Code.:

Synonyms:diphenyloctylgermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyloctylgermane

Chemical Property:

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Technology Process of diphenyloctylgermane

There total 5 articles about diphenyloctylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.1%

: 100184-62-1
Diphenyloctylbromogermane

: 100184-63-2
diphenyloctylgermane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 3h; Heating;
DOI:10.1246/bcsj.58.1443

Reference yield: 38.1%

: 16853-85-3
lithium aluminium tetrahydride

: 100184-62-1
Diphenyloctylbromogermane

: 100184-63-2
diphenyloctylgermane

Guidance literature:: In diethyl ether; mixt. of Ph2Ge(Br)C8H17 and LiAlH4 in ether stirred with reflux for 3 h, hydrolyzed; org. layer dried over CaCl2, evapd., fractionally distd.; elem. anal.;
DOI:10.1246/bcsj.58.1443

Reference yield: 38.0%

: 100184-59-6
diphenylgermylenedipotassium

: 111-83-1
1-bromo-octane

: 111-65-9
octane

: 1675-58-7
diphenylgermane

: 100184-63-2
diphenyloctylgermane

: 4237-11-0
Dioctyl-diphenyl-germane

Guidance literature:: With water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to n-C8H17Br, stirred at room temp. for 30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
DOI:10.1246/bcsj.58.1443