diphenylgermylenedipotassium

Base Information

Chemical Name:diphenylgermylenedipotassium
CAS No.:100184-59-6
Molecular Formula:C₁₂H₁₀GeK₂
Molecular Weight:304.998
Hs Code.:

Synonyms:diphenylgermylenedipotassium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenylgermylenedipotassium

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of diphenylgermylenedipotassium

There total 1 articles about diphenylgermylenedipotassium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1675-58-7
diphenylgermane

: 100184-59-6
diphenylgermylenedipotassium

Guidance literature:: With potassium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; under Ar, small pieces of K stirred vigorously in anhyd. HMPA and THF, Ph2GeH2 in THF added dropwise, reacted for about 40 min; not isolated; determined by hydrolysis with D2O;
DOI:10.1246/bcsj.58.1443

Reference yield: 82.8%

: 100184-59-6
diphenylgermylenedipotassium

: 75-29-6
isopropyl chloride

: (C₆H₅)2Ge(CH(CH₃)2)2

: 1675-58-7
diphenylgermane

: 100184-64-3
Isopropyldiphenylgermane

Guidance literature:: With water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to i-PrCl, stirred at room temp. for30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
DOI:10.1246/bcsj.58.1443

Reference yield: 60.3%

: 100184-59-6
diphenylgermylenedipotassium

: 100-44-7
benzyl chloride

: benzyldiphenylgermane

: 1675-58-7
diphenylgermane

: 100184-65-4
Dibenzyldiphenylgermane

: 108-88-3,15644-74-3,16713-13-6
toluene

Guidance literature:: With water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to PhCH2Cl, stirred at room temp. for 30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
DOI:10.1246/bcsj.58.1443