tetrabutylammonium bis(pentachlorophenyl)silver(I)

Base Information

Chemical Name:tetrabutylammonium bis(pentachlorophenyl)silver(I)
CAS No.:86722-05-6
Molecular Formula:C₁₂AgCl₁₀*C₁₆H₃₆N
Molecular Weight:848.999
Hs Code.:

Synonyms:tetrabutylammonium bis(pentachlorophenyl)silver(I)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrabutylammonium bis(pentachlorophenyl)silver(I)

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Technology Process of tetrabutylammonium bis(pentachlorophenyl)silver(I)

There total 1 articles about tetrabutylammonium bis(pentachlorophenyl)silver(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 2966-50-9
silver trifluoroacetate

: 6782-80-5
pentachlorophenyllithium

: 39481-22-6
tetrabutylammonium trifluoroacetate

: 86722-05-6
tetrabutylammonium bis(pentachlorophenyl)silver(I)

Guidance literature:: In diethyl ether; to ether soln. of LiC6Cl5 at -20°C added CF3COOAg, stirred for 15 min, (Bu4N)O2CCF3 added, stirred for 1 h at -20°C, allowed to warm to room temp. (2 h); ppt. filtered off, washed with water, extd. with CH2Cl2, filtered, concd., ether added; elem. anal.;
DOI:10.1016/S0022-328X(00)98739-4

Reference yield: 87.0%

: 86722-05-6
tetrabutylammonium bis(pentachlorophenyl)silver(I)

: 76-05-1
trifluoroacetic acid

: (C₄H₉)4N⁽¹⁺⁾*[Ag(C₆Cl₅)(CF₃COO)]^(1-)=(C₄H₉)4N[Ag(C₆Cl₅)(CF₃COO)]

Guidance literature:: In diethyl ether; CF3COOH added to suspn. of Ag complex in Et2O, stirred for 45 min at room temp.; concn., stirring for 5 h at -20°C, filtration; elem. anal.;
DOI:10.1016/S0022-328X(00)98739-4

Reference yield: 87.0%

: 148-24-3,24804-14-6
8-quinolinol

: 86722-05-6
tetrabutylammonium bis(pentachlorophenyl)silver(I)

: 86722-15-8
Bu₄N[Ag(C₆Cl₅)(8-oxyquinolato)]

Guidance literature:: In diethyl ether; 8-hydroxyquinoline added to suspn. of Ag complex in Et2O, stirred for 45 min at room temp.; concn., stirring for 5 h at -20°C, filtration; elem. anal.;
DOI:10.1016/S0022-328X(00)98739-4