(4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride

Base Information

Chemical Name:(4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride
CAS No.:147907-34-4
Molecular Formula:C₁₁H₁₅ClNO₄P
Molecular Weight:291.671
Hs Code.:

Synonyms:(4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride

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Chemical Property of (4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride

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Technology Process of (4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride

There total 3 articles about (4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2491-20-5
L-alanine methyl ester hydrochloride

: 878-17-1
4-methylphenyl phosphorodichloridate

: 147907-34-4
(4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride

Guidance literature:: With triethylamine; In dichloromethane; at -70 - 20 ℃; for 6h;
DOI:10.1021/jm00060a013

Reference yield:

: 106-44-5
p-cresol

: 147907-34-4
(4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / triethylamine, phosphoryl chloride / diethyl ether / 1.) from 0 deg C to RT, 15 h, 2.) reflux, 2h

2: 100 percent / triethylamine / CH₂Cl₂ / 6 h / -70 - 20 °C

With triethylamine; trichlorophosphate; In diethyl ether; dichloromethane;
DOI:10.1021/jm00060a013

Reference yield:

: 106-44-5
p-cresol

: 147907-34-4
(4-methylphenoxy) ((1S)-(1-methoxycarbonylethyl)amino)phosphinyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate; triethylamine / diethyl ether / -78 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 2 h / -78 - 20 °C

With triethylamine; trichlorophosphate; In diethyl ether; dichloromethane;