(2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine

Base Information

Chemical Name:(2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine
CAS No.:1332503-95-3
Molecular Formula:C₁₈H₃₃NO₂SSi
Molecular Weight:355.617
Hs Code.:

Synonyms:(2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine

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Technology Process of (2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine

There total 4 articles about (2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1332503-94-2
(S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylthio)-butan-2-amine

: 1332503-95-3
(2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine

Guidance literature:: With sodium periodate; In methanol; water; ethyl acetate; at 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/jo201341q

Reference yield:

: 2899-37-8
(S)-methioninol

: 1332503-95-3
(2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 2 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: 1H-imidazole / dichloromethane / 2 h / Inert atmosphere

3.1: sodium periodate / methanol; water; ethyl acetate / 3.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; sodium periodate; In methanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/jo201341q

Reference yield:

: 63-68-3,26062-47-5,58576-49-1
L-methionine

: 1332503-95-3
(2S)-N-benzyl-1-(tert-butyldimethylsilyloxy)-4-(methylsulfinyl)butan-2-amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / Reflux; Inert atmosphere

2.1: methanol / 2 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 °C / Inert atmosphere

3.1: 1H-imidazole / dichloromethane / 2 h / Inert atmosphere

4.1: sodium periodate / methanol; water; ethyl acetate / 3.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; sodium periodate; lithium aluminium tetrahydride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/jo201341q