N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole

Base Information

Chemical Name:N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole
CAS No.:861622-66-4
Molecular Formula:C₁₄H₂₁N
Molecular Weight:203.327
Hs Code.:

Synonyms:N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole

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Technology Process of N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole

There total 3 articles about N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 146900-30-3
dodecahydro-N-ethyl-1H-carbazole

: 26727-32-2
2,3,4,5,6,7,8,9-octahydro-1H-carbazole

: 861622-66-4
N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole

Guidance literature:: With chlorohydrido(2,6-bis(di-tert-butylphosphinito)phen-1-yl)iridium(III); sodium t-butanolate; at 178 ℃; for 48h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c4cc02073a

Reference yield: 48.0%

: 146900-30-3
dodecahydro-N-ethyl-1H-carbazole

: 861622-66-4
N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole

: 86-28-2
N-ethylcarbazole

Guidance literature:: With RhCl(CO)(PMe₃)2; for 3h; Overall yield = 80 %; Irradiation; Inert atmosphere;

Reference yield:

: 86-28-2
N-ethylcarbazole

: 26727-32-2
2,3,4,5,6,7,8,9-octahydro-1H-carbazole

: 861622-66-4
N-ethyl-1,2,3,4,5,6,7,8-octahydrocarbazole

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / 48 h / 120 °C

2: sodium t-butanolate; chlorohydrido(2,6-bis(di-tert-butylphosphinito)phen-1-yl)iridium(III) / 48 h / 178 °C / Schlenk technique; Inert atmosphere

With chlorohydrido(2,6-bis(di-tert-butylphosphinito)phen-1-yl)iridium(III); palladium on activated charcoal; hydrogen; sodium t-butanolate;
DOI:10.1039/c4cc02073a