Dicyclohexyl[(1Z)-1-(trimethylsilyl)-1-hexen-1-yl]borane

Base Information

Chemical Name:Dicyclohexyl[(1Z)-1-(trimethylsilyl)-1-hexen-1-yl]borane
CAS No.:338999-00-1
Molecular Formula:C₂₁H₄₁BSi
Molecular Weight:332.453
Hs Code.:
DSSTox Substance ID:DTXSID701202595
Nikkaji Number:J2.339.258E

Synonyms:DTXSID701202595;338999-00-1;Dicyclohexyl[(1Z)-1-(trimethylsilyl)-1-hexen-1-yl]borane

Suppliers and Price of Dicyclohexyl[(1Z)-1-(trimethylsilyl)-1-hexen-1-yl]borane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Dicyclohexyl[(1Z)-1-(trimethylsilyl)-1-hexen-1-yl]borane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:7
Exact Mass:332.3070580
Heavy Atom Count:23
Complexity:339

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B(C1CCCCC1)(C2CCCCC2)C(=CCCCC)[Si](C)(C)C
Isomeric SMILES:B(C1CCCCC1)(C2CCCCC2)/C(=C/CCCC)/[Si](C)(C)C

Technology Process of Dicyclohexyl[(1Z)-1-(trimethylsilyl)-1-hexen-1-yl]borane

There total 5 articles about Dicyclohexyl[(1Z)-1-(trimethylsilyl)-1-hexen-1-yl]borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3844-94-8
1-(trimethylsilyl)-1-hexyne

: 1568-65-6
bis(cyclohexanyl)borane

: 338999-00-1
dicyclohexyl[(Z)-1-(trimethylsilyl)hex-1-enyl]borane

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1016/S0040-4039(03)01750-7

Reference yield:

: 110-83-8
cyclohexene

: 338999-00-1
dicyclohexyl[(Z)-1-(trimethylsilyl)hex-1-enyl]borane

Guidance literature:: Multi-step reaction with 2 steps

1: BH₃ / tetrahydrofuran / 2 h / 0 °C

2: tetrahydrofuran / 2 h / 0 °C

With borane; In tetrahydrofuran;
DOI:10.1055/s-2006-942373

Reference yield:

: 693-02-7
hex-1-yne

: 338999-00-1
dicyclohexyl[(Z)-1-(trimethylsilyl)hex-1-enyl]borane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / 1 h / -78 °C

1.2: 1 h / -78 °C

2.1: tetrahydrofuran / 3 h / 0 °C

With n-butyllithium; In tetrahydrofuran;
DOI:10.1016/S0040-4039(03)01750-7